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2 edition of Synthesis of compounds from butan-2,3-dione found in the catalog.

Synthesis of compounds from butan-2,3-dione

Ioanna Alexandropolou

Synthesis of compounds from butan-2,3-dione

by Ioanna Alexandropolou

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Published by University of Portsmouth, School of Pharmacy, Biomedical and Physical Sciences in Portsmouth .
Written in English


Edition Notes

Thesis (Ph.D.) - University of Portsmouth, 1997.

Statementby Ioanna Alexandropolou.
ID Numbers
Open LibraryOL16826097M

  Introduction []. Synthetic chemists are interested in a variety of information when planning a synthesis. That may include the conditions under which the reaction is to occur, the starting materials and reagents, catalysts, reaction sites, yields, products, by-products, functional group transformations, bonding changes, and mechanisms of the :// 3,5-disec-butyl-1,2-cyclohexanedione - C14H24O2, synthesis, structure, density, melting point, boiling point

A Convinent Route for Synthesis of New Stable 1, 4-Diionic Compounds from Three Component Reactiones of 4, 4, 4-Trifluorothiophenyl-butan-1, 3-dione, Dialkyl K Pourshamsian, N Montazeri, S Ali-Asgari, MM Zeydi, E Biazar?user=kLcrYp4AAAAJ&hl=en. Abstract. Aromadendranes (1) belong to a class of sesquiterpenes, structurally characterized by a dimethyl cyclopropane ring fused to a hydroazulene skeleton, as depicted in Fig. hout this and the following sections the numbering of the carbon skeleton will be used as given in (1).Next to the aromadendranes, the related sesquiterpenes with a 1,7-cycloaromadendrane, 7,8-seco-, and 9,10

  2,2,4,4,4-pentafluoro-3,3-dihydroxy(thiophenyl)butanone (4b) The title compound was prepared according to General Procedure B from 4,4,4-trifluoro(thiophenyl)butane-1,3-dione ( g, 5 mmol) and SelectfluorTM ( g, mmol) in acetonitrile (20 ml), without further purification to give a dark brown solid ( g, % yield). Symbol which looks like a small house Solid circle with an upward pointer in it. Jump to content?ID=C&Mask=


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Synthesis of compounds from butan-2,3-dione by Ioanna Alexandropolou Download PDF EPUB FB2

5-Trifluoromethoxy-1H-indole-2,3-dione 3-(N-ethyl/benzylthiosemicarbazone) (2a/2b) and 5-trifluoromethoxymorpholinomethyl-1H-indole-2,3-dione 3-(N-ethylthiosemicarbazone) (3a) were structures of the compounds were confirmed by elemental analysis, spectral data and X-ray single crystal diffraction :// Quinoxaline-2, 3-dione obtained from cyclocondensation reaction of o-phenylene diamine with oxalic acid was reacted with three different ketones and formaldehyde to give the corresponding Mannich bases in satisfactory yield.

Their structures were confirmed by using 1 Synthesis of compounds from butan-2,3-dione book NMR, IR, and mass analysis. In pharmacological evaluation, the synthesized compounds showed its curative effect against   Abstract: Quinoxaline-2, 3-dione obtained from cyclocondensation reaction of o-phenylene diamine with oxalic acid, was reacted with chlorosulphonic acid under cold condition followed by a reaction with various benzimidazoles to give 2, 3- dioxo-1, 2, 3, 4-tetrahydroquinoxalinesulphonyl benzimidazoles in satisfactory Download Citation | Design and Synthesis of Pyrano[2,3- a ]carbazoles by Multicomponent Reaction | A facile, efficient, three-component reaction of 2,3,4,9-tetrahydro-1H-carbazolone Search results for butane-2,3-dione at Sigma-Aldrich.

Compare Products: Select up to 4 products. *Please select more than one item to compare?term=butane-2,3-dione&interface=All&N=0. E/Z-1,1,1-trifluoromethoxymethyl(thienyl)butenone by vacuumfiltration of the resulting reaction mixture were unsuccessful because without the use of ethyl etherasacarriersolvent,theyieldwasverylowandacom-plex mixture of products including 2 and 3 was obtained.

When ethyl ether was used as a carrier solvent, the yield of Novel non-planar heterocycles make a great contribution to drug design and medicinal chemistry. Fused aryl[e][1,3]diazepinediones are a less investigated and appealing class of compounds. Herein, we designed 5 types of polynitrogen containing compounds based on 3-aminobenzo[e][1,3]diazepine-1,5-dione This book aims to overview the role of non-covalent interactions, such as hydrogen and halogen bonding, π-π, π-anion and electrostatic interactions, hydrophobic effects and van der Waals forces in the synthesis of organic and inorganic compounds, as well as in design of new crystals and function proposed book should allow to combine, in a systematic way, recent advances on the 3-Phenyl-4,5-diaminoisoxazole hydrochloride (69) reacted with isoamyl nitrite in THF to afford the diazo compound (70), which underwent immediate closure on treatment with aqueous base (5% NaOH) to furnish 3-phenylisoxazolo[4,5-d]-1,2,3-triazole (71).The isoxazolotriazole, which resulted in essentially quantitative yield, is a relatively stable compound 〈70T〉.

First-principles study on the gas-phase decomposition of bio-oil oxygenated compounds over the palladium catalyst surface namely, 2-butenal, butan-2,3-diol, and butan-2,3-dione were considered as the representative compounds of the oxygenated catalogue of bio-oils.

The decomposition mechanisms of these model compounds along with #. 3,6‐Dicyano‐4,5‐benzotricyclo[ 3,8]‐4‐nonene 6,7‐Dimethoxycoumarin Photochemical Key Steps in Organic Synthesis: An Experimental Course Book In the title compound, 3-[(2-acetamido­phen­yl)imino]­butanone, C12H14N2O2, the imine C=N bond is essentially coplanar with the ketone C=O bond in an s-trans conformation.

The benzene ring is twisted away from the plane of the C=N bond by (14)°. The acetamido unit is essentially coplanar with the benzene ring. In the crystal, mol­ecules are connected into chains along the c axis The reaction sequences for the synthesis of coumarins 2–11 starting from 4-hydroxycoumarin are outlined in Scheme 2-(coumarinyloxy)acetate (1) was obtained by refluxing methyl bromoacetate with 4-hydroxycoumarin in anhydrous acetone in the presence of anhydrous potassium FT-IR spectrum of this compound showed an absorption band at 1, cm −1 (ester 3,4-Dihydroxycyclobutene-1,2-dione ≥% (HPLC) Synonym: Squaric acid CAS Number Linear Formula (HO) 2 C 4 (=O) 2.

Molecular Weight Beilstein/REAXYS Number EC Number MDL number MFCD PubChem Substance ID NACRES NA   Abstract The synthesis of 2,3,4,5 tetrasubstituted and 2,3,5-trisubstituted furans from suitable butan-1,4-dione derivatives is described.

Furan Derivatives from Cyclodehydratign of Brackein-Like 1,4-Dicarbonyl Compounds: Synthetic Communications: No There are few examples of the [3+1] two-fragment cyclization reactions and of transformations from four-membered rings to seven-membered ones.

These methods are rather limited in scope, because they are only for the synthesis of particular compounds, for example, 2,8-dihalothia-tricyclo[ 3,6]://   Supporting Information Design of High Performance Photoinitiators at nm: Search around the Naphthalene Scaffold.

Pu Xiao,a Frédéric Dumur,b,c,d Bernadette Graff,a Fabrice Morlet-Savary,a Didier Gigmes,*,b Jean Pierre Fouassier 1 and Jacques Lalevée*,a aInstitut de Science des Matériaux de Mulhouse IS2M, UMR CNRSUHA, 15, rue Jean Synthesis and study of macroheterocyclic compounds derived from 1 H -phenalene-1,3(2 H)-diimine August Russian Journal of General Chemistry 74(8) Arduini, Arturo; Pochini, Andrea; Ungaro, Rocco: Selective Synthesis of 2-Alkenylphenols and 2,2-Dialkyl-2,3-dihydrobenzofurans from 2-Hydroxybenzyl Alcohols Full Text PDF ( kb) Book Series Help; Contact Portal SYNTHESIS The Cyclodesulfurization of Thio Compounds; VII.

A New Facile Synthesis of N Synthesis of 1,2-Diphenylcyclobutene-3,4-dione Full Text PDF ( kb) 47 CLARK, Robin D.; HEATHCOCK, Clayton H.:.

A direct asymmetric hydrogenation of unprotected enamino esters and amides is described. Catalyzed by Rh complexes with Josiphos-type chiral ligands, this method gives β-amino esters and amides in high yield and high ee (93−97% ee).

No acyl protection/deprotection is UDC + Oxidative methods in the synthesis of vicinal di- and polycarbonyl compounds V D Filimonov, M S Yusubov, Ki-Van Chi Contents I. Introduction II. Oxidation of carbonyl compounds and their derivatives III.

Oxidation of 1,2-diols, epoxides and other vicinally substituted compounds A novel approach for the synthesis of unsymmetrically substituted dibenzo[b,f][1,5]diazocine-6,12(5H,11H)diones has been facile three-step method uses variously substituted 1H-benzo[d][1,3]oxazine-2,4-diones (isatoic anhydrides) and 2-aminobenzoic acids as a starting obtained products were further transformed into N-alkyl- N-acetyl- and dithio ://